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Laboratory

Our labs are equipped with nanostructure synthesis tools, morphological, electronic, and chemical characterization under ultrahigh vacuum (UHV) and atmospheric pressure conditions.

System 1: UHV surface science / nanocluster catalysis system (SPECS GmbH).

These modular system consists of four UHV-chambers: a surface analysis chamber, a scanning tunneling microscopy chamber (variable temperature STM), a sample preparation chamber, and a load lock chamber for quick sample transfer into UHV. The components that are present in the chambers are detailed below. Also available: an overview of the system, a view of the chamber design, and a series of pictures taken during the installation phase.

Luis Ono, Abhilash Vincent, and Prof. Roldan

Sample preparation chamber:

  • 4-pocket electron beam evaporator with flux monitor (Oxford Sci.) for in-situ metal growth.
  • Dual Knudsen-cell evaporator for in-situ growth of bimetallic alloys.
  • Quartz microbalance that monitors thickness during evaporation.
  • Hybrid atom/ion Plasma source (Oxford Sci.) for H2, O2, N2 controlled production of ultrathin metal oxide films and removal of residual organics resulting from ex-situ nanoparticle synthesis.
  • Argon sputter gun for sample cleaning.
  • Mass spectrometer for rest gas analysis.

Surface analysis chamber:

  • Hemispherical electron energy analyzer
  • Non-monochromatic (Al/Mg anodes) and monochromatic (Al/Ag anodes) X-ray sources for X-ray Photoelectron Spectroscopy (XPS) for characterization of chemical composition and electronic properties of nanomaterials.
  • Electron source (EQ 22/35, SPECS) for Auger Electron Spectroscopy (AES).
  • Ultraviolet Source for Ultraviolet Photoelectron Spectroscopy (UPS).
  • Mass spectrometer (HIDEN) for Temperature-Programmed Desorption (TPD).
  • Low Energy Electron Diffraction (LEED) for characterazing the crystalline structure of surfaces.
  • Gas manifold allowing four different gases and one vaporized liquid to be simultaneously injected into the analysis chamber.
  • Nanosecond YAG laser: 355 nm, 532 nm, 1064 nm (EKSPLA) for in-situ nanoparticle melting and re-shaping.

Scanning Tunneling Microscopy chamber:

  • Variable Temperature Scanning Tunneling microscope (Aarhus-SPECS)
  • Parking station with heating capabilities
  • Argon sputter gun for tip cleaning.




UHV system 1 (SPECS) in Roldan's laboratory.



The original system design - a joint effort between Prof. Roldan and SPECS


UHV-System 1 featuring in-situ laser-induced nanoparticle re-shaping


System 2: UHV microscopy system

The system includes a room temperature UHV AFM/STM (Omicron) and a load-lock chamber for quick sample transfer. An in-situ magneto-optic Kerr effect setup for the analysis chamber is under construction.


UHV-System 2 installed in Prof. Roldan's lab featuring in-situ AFM/STM


System 3: Microreactor and integrated mass spectrometer system (HIDEN)

A home-built microreactor interfaced with a commercial high pressure mass spectrometer system is available for the rapid screening of catalytic activity. This system allows real-time continuous analysis of multiple gas components.

  • Microreactor: gas manifold with independent inlets for four gases and a vaporized liquid (mass flow controlled) and a high temperature quartz reactor column for easy-access catalyst placement with minimal changeover time. The sample temperature can be tuned within the range of ambient to 600C and an "in-bed" thermocouple is available.

  • Mass Spectrometer (HPR20, HIDEN): Detection of the gases/vapors used or generated in the microreactor can be performed with high sensitivity and fast response using a compact bench top mass spectrometer system (200 amu mass range dual Faraday/Electron multiplier detector) configured for continuous gas analysis in the pressure range 10 mTorr to 2 bar.


Microreactor with integrated mass spectrometer